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Description
Additively Manufactured Thin-wall Inconel 718 specimens commonly find application in heat exchangers and Thermal Protection Systems (TPS) for space vehicles. The wall thicknesses in applications for these components typically range between 0.03-2.5mm. Laser Powder Bed Fusion (PBF) Fatigue standards assume thickness over 5mm and consider Hot Isostatic Pressing

Additively Manufactured Thin-wall Inconel 718 specimens commonly find application in heat exchangers and Thermal Protection Systems (TPS) for space vehicles. The wall thicknesses in applications for these components typically range between 0.03-2.5mm. Laser Powder Bed Fusion (PBF) Fatigue standards assume thickness over 5mm and consider Hot Isostatic Pressing (HIP) as conventional heat treatment. This study aims at investigating the dependence of High Cycle Fatigue (HCF) behavior on wall thickness and Hot Isostatic Pressing (HIP) for as-built Additively Manufactured Thin Wall Inconel 718 alloys. To address this aim, high cycle fatigue tests were performed on specimens of seven different thicknesses (0.3mm,0.35mm, 0.5mm, 0.75mm, 1mm, 1.5mm, and 2mm) using a Servohydraulic FatigueTesting Machine. Only half of the specimen underwent HIP, creating data for bothHIP and No-HIP specimens. Upon analyzing the collected data, it was noticed that the specimens that underwent HIP had similar fatigue behavior to that of sheet metal specimens. In addition, it was also noticed that the presence of Porosity in No-HIP specimens makes them more sensitive to changes in stress. A clear decrease in fatigue strength with the decrease in thickness was observed for all specimens.
ContributorsSaxena, Anushree (Author) / Bhate, Dhruv (Thesis advisor) / Liu, Yongming (Committee member) / Kwon, Beomjin (Committee member) / Arizona State University (Publisher)
Created2021
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Description
Laser powder bed fusion (LPBF) additive manufacturing (AM) has received widespread attention due to its ability to produce parts with complicated design and better surface finish compared to other additive techniques. LPBF uses a laser heat source to melt layers of powder particles and manufactures a part based on the

Laser powder bed fusion (LPBF) additive manufacturing (AM) has received widespread attention due to its ability to produce parts with complicated design and better surface finish compared to other additive techniques. LPBF uses a laser heat source to melt layers of powder particles and manufactures a part based on the CAD design. This process can benefit significantly through computational modeling. The objective of this thesis was to understand the thermal transport, and fluid flow phenomena of the process, and to optimize the main process parameters such as laser power and scan speed through a combination of computational, experimental, and statistical analysis. A multi-physics model was built using to model temperature profile, bead geometry and elemental evaporation in powder bed process using a non-gaussian interaction between laser heat source and metallic powder. Owing to the scarcity of thermo-physical properties of metallic powders in literature, thermal conductivity, diffusivity, and heat capacity was experimentally tested up to a temperature of 1400 degrees C. The values were used in the computational model, which improved the results significantly. The computational work was also used to assess the impact of fluid flow around melt pool. Dimensional analysis was conducted to determine heat transport mode at various laser power/scan speed combinations. Convective heat flow proved to be the dominant form of heat transfer at higher energy input due to violent flow of the fluid around the molten region, which can also create keyhole effect. The last part of the thesis focused on gaining useful information about several features of the bead area such as contact angle, porosity, voids and melt pool that were obtained using several combinations of laser power and scan speed. These features were quantified using process learning, which was then used to conduct a full factorial design that allows to estimate the effect of the process parameters on the output features. Both single and multi-response analysis are applied to analyze the output response. It was observed that laser power has more influential effect on all the features. Multi response analysis showed 150 W laser power and 200 mm/s produced bead with best possible features.
ContributorsAhsan, Faiyaz (Author) / Ladani, Leila (Thesis advisor) / Razmi, Jafar (Committee member) / Kwon, Beomjin (Committee member) / Nian, Qiong (Committee member) / Zhuang, Houlong (Committee member) / Arizona State University (Publisher)
Created2021
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Description
Applications such as heat exchangers, surface-based cellular structures, rotating blades, and waveguides rely on thin metal walls as crucial constituent elements of the structure. The design freedom enabled by laser powder bed fusion has led to an interest in exploiting this technology to further the performance of these components, many

Applications such as heat exchangers, surface-based cellular structures, rotating blades, and waveguides rely on thin metal walls as crucial constituent elements of the structure. The design freedom enabled by laser powder bed fusion has led to an interest in exploiting this technology to further the performance of these components, many of which retain their as-built surface morphologies on account of their design complexity. However, there is limited understanding of how and why mechanical properties vary by wall thickness for specimens that are additively manufactured and maintain an as-printed surface finish. Critically, the contributions of microstructure and morphology to the mechanical behavior of thin wall laser powder bed fusion structures have yet to be systematically identified and decoupled. This work focuses on elucidating the room temperature quasi-static tensile and high cycle fatigue properties of as-printed, thin-wall Inconel 718 fabricated using laser powder bed fusion, with the aim of addressing this critical gap in the literature. Wall thicknesses studied range from 0.3 - 2.0 mm, and the effects of Hot Isostatic Pressing are also examined, with sheet metal specimens used as a baseline for comparison. Statistical analyses are conducted to identify the significance of the dependence of properties on wall thickness and Hot Isostatic Pressing, as well as to examine correlations of these properties to section area, porosity, and surface roughness. A thorough microstructural study is complemented with a first-of-its-kind study of surface morphology to decouple their contributions and identify underlying causes for observed changes in mechanical properties. This thesis finds that mechanical properties in the quasi-static and fatigue framework do not see appreciable declines until specimen thickness is under 0.75 mm in thickness. The added Hot Isostatic Pressing heat treatment effectively closed pores, recrystallized the grain structure, and provided a more homogenous microstructure that benefits the modulus, tensile strength, elongation, and fatigue performance at higher stresses. Stress heterogeneities, primarily caused by surface defects, negatively affected the thinner specimens disproportionately. Without the use of the Hot Isostatic Pressing, the grain structure remained much more refined and benefitted the yield strength and fatigue endurance limit.
ContributorsParadise, Paul David (Author) / Bhate, Dhruv (Thesis advisor) / Chawla, Nikhilesh (Committee member) / Azeredo, Bruno (Committee member) / Jiao, Yang (Committee member) / Arizona State University (Publisher)
Created2022
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Description
High-temperature mechanical behaviors of metal alloys and underlying microstructural variations responsible for such behaviors are essential areas of interest for many industries, particularly for applications such as jet engines. Anisotropic grain structures, change of preferred grain orientation, and other transformations of grains occur both during metal powder bed fusion additive

High-temperature mechanical behaviors of metal alloys and underlying microstructural variations responsible for such behaviors are essential areas of interest for many industries, particularly for applications such as jet engines. Anisotropic grain structures, change of preferred grain orientation, and other transformations of grains occur both during metal powder bed fusion additive manufacturing processes, due to variation of thermal gradient and cooling rates, and afterward during different thermomechanical loads, which parts experience in their specific applications, could also impact its mechanical properties both at room and high temperatures. In this study, an in-depth analysis of how different microstructural features, such as crystallographic texture, grain size, grain boundary misorientation angles, and inherent defects, as byproducts of electron beam powder bed fusion (EB-PBF) AM process, impact its anisotropic mechanical behaviors and softening behaviors due to interacting mechanisms. Mechanical testing is conducted for EB-PBF Ti6Al4V parts made at different build orientations up to 600°C temperature. Microstructural analysis using electron backscattered diffraction (EBSD) is conducted on samples before and after mechanical testing to understand the interacting impact that temperature and mechanical load have on the activation of certain mechanisms. The vertical samples showed larger grain sizes, with an average of 6.6 µm, a lower average misorientation angle, and subsequently lower strength values than the other two horizontal samples. Among the three strong preferred grain orientations of the α phases, <1 1 2 ̅ 1> and <1 1 2 ̅ 0> were dominant in horizontally built samples, whereas the <0 0 0 1> was dominant in vertically built samples. Thus, strong microstructural variation, as observed among different EB-PBF Ti6Al4V samples, mainly resulted in anisotropic behaviors. Furthermore, alpha grain showed a significant increase in average grain size for all samples with the increasing test temperature, especially from 400°C to 600°C, indicating grain growth and coarsening as potential softening mechanisms along with temperature-induced possible dislocation motion. The severity of internal and external defects on fatigue strength has been evaluated non-destructively using quantitative methods, i.e., Murakami’s square root of area parameter model and Basquin’s model, and the external surface defects were rendered to be more critical as potential crack initiation sites.
ContributorsMian, Md Jamal (Author) / Ladani, Leila (Thesis advisor) / Razmi, Jafar (Committee member) / Shuaib, Abdelrahman (Committee member) / Mobasher, Barzin (Committee member) / Nian, Qiong (Committee member) / Arizona State University (Publisher)
Created2022
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Description
The design of energy absorbing structures is driven by application specific requirements like the amount of energy to be absorbed, maximum transmitted stress that is permissible, stroke length, and available enclosing space. Cellular structures like foams are commonly leveraged in nature for energy absorption and have also found use in

The design of energy absorbing structures is driven by application specific requirements like the amount of energy to be absorbed, maximum transmitted stress that is permissible, stroke length, and available enclosing space. Cellular structures like foams are commonly leveraged in nature for energy absorption and have also found use in engineering applications. With the possibility of manufacturing complex cellular shapes using additive manufacturing technologies, there is an opportunity to explore new topologies that improve energy absorption performance. This thesis aims to systematically understand the relationships between four key elements: (i) unit cell topology, (ii) material composition, (iii) relative density, and (iv) fields; and energy absorption behavior, and then leverage this understanding to develop, implement and validate a methodology to design the ideal cellular structure energy absorber. After a review of the literature in the domain of additively manufactured cellular materials for energy absorption, results from quasi-static compression of six cellular structures (hexagonal honeycomb, auxetic and Voronoi lattice, and diamond, Gyroid, and Schwarz-P) manufactured out of AlSi10Mg and Nylon-12. These cellular structures were compared to each other in the context of four design-relevant metrics to understand the influence of cell design on the deformation and failure behavior. Three new and revised metrics for energy absorption were proposed to enable more meaningful comparisons and subsequent design selection. Triply Periodic Minimal Surface (TPMS) structures were found to have the most promising overall performance and formed the basis for the numerical investigation of the effect of fields on the energy absorption performance of TPMS structures. A continuum shell-based methodology was developed to analyze the large deformation behavior of field-driven variable thickness TPMS structures and validated against experimental data. A range of analytical and stochastic fields were then evaluated that modified the TPMS structure, some of which were found to be effective in enhancing energy absorption behavior in the structures while retaining the same relative density. Combining findings from studies on the role of cell geometry, composition, relative density, and fields, this thesis concludes with the development of a design framework that can enable the formulation of cellular material energy absorbers with idealized behavior.
ContributorsShinde, Mandar (Author) / Bhate, Dhruv (Thesis advisor) / Peralta, Pedro (Committee member) / Liu, Yongming (Committee member) / Jiao, Yang (Committee member) / Kwon, Beomjin (Committee member) / Arizona State University (Publisher)
Created2023
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Description
Additive manufacturing (AM) has been extensively investigated in recent years to explore its application in a wide range of engineering functionalities, such as mechanical, acoustic, thermal, and electrical properties. The proposed study focuses on the data-driven approach to predict the mechanical properties of additively manufactured metals, specifically Ti-6Al-4V. Extensive data

Additive manufacturing (AM) has been extensively investigated in recent years to explore its application in a wide range of engineering functionalities, such as mechanical, acoustic, thermal, and electrical properties. The proposed study focuses on the data-driven approach to predict the mechanical properties of additively manufactured metals, specifically Ti-6Al-4V. Extensive data for Ti-6Al-4V using three different Powder Bed Fusion (PBF) additive manufacturing processes: Selective Laser Melting (SLM), Electron Beam Melting (EBM), and Direct Metal Laser Sintering (DMLS) are collected from the open literature. The data is used to develop models to estimate the mechanical properties of Ti-6Al-4V. For this purpose, two models are developed which relate the fabrication process parameters to the static and fatigue properties of the AM Ti-6Al-4V. To identify the behavior of the relationship between the input and output parameters, each of the models is developed on both linear multi-regression analysis and non-linear Artificial Neural Network (ANN) based on Bayesian regularization. Uncertainties associated with the performance prediction and sensitivity with respect to processing parameters are investigated. Extensive sensitivity studies are performed to identify the important factors for future optimal design. Some conclusions and future work are drawn based on the proposed study with investigated material.
ContributorsSharma, Antriksh (Author) / Liu, Yongming (Thesis advisor) / Nian, Qiong (Committee member) / Jiao, Yang (Committee member) / Arizona State University (Publisher)
Created2020
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Description
One of the fundamental aspects of cellular material design is cell shape selection. Of particular interest is how this selection can be made in the context of a realistic three-dimensional structure. Towards this goal, this work studied the stiffness response of periodic and stochastic lattice structures for the loading conditions

One of the fundamental aspects of cellular material design is cell shape selection. Of particular interest is how this selection can be made in the context of a realistic three-dimensional structure. Towards this goal, this work studied the stiffness response of periodic and stochastic lattice structures for the loading conditions of bending, torsion and tension/compression using commercially available lattice design optimization software. The goal of this computational study was to examine the feasibility of developing a ranking order based on minimum compliance or maximum stiffness for enabling cell selection. A study of stochastic shapes with different seeds was also performed. Experimental compression testing was also performed to validate a sample space of the simulations. The findings of this study suggest that under certain circumstances, stochastic shapes have the potential to generate the highest stiffness-to-weight ratio in the test environments considered.
ContributorsSharma, Raghav (Author) / Bhate, Dhruv (Thesis advisor) / Oswald, Jay (Committee member) / Kwon, Beomjin (Committee member) / Arizona State University (Publisher)
Created2019
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Description
This dissertation aims at developing novel materials and processing routes using alkali activated aluminosilicate binders for porous (lightweight) geopolymer matrices and 3D-printing concrete applications. The major research objectives are executed in different stages. Stage 1 includes developing synthesis routes, microstructural characterization, and performance characterization of a family of economical, multifunctional

This dissertation aims at developing novel materials and processing routes using alkali activated aluminosilicate binders for porous (lightweight) geopolymer matrices and 3D-printing concrete applications. The major research objectives are executed in different stages. Stage 1 includes developing synthesis routes, microstructural characterization, and performance characterization of a family of economical, multifunctional porous ceramics developed through geopolymerization of an abundant volcanic tuff (aluminosilicate mineral) as the primary source material. Metakaolin, silica fume, alumina powder, and pure silicon powder are also used as additional ingredients when necessary and activated by potassium-based alkaline agents. In Stage 2, a processing route was developed to synthesize lightweight geopolymer matrices from fly ash through carbonate-based activation. Sodium carbonate (Na2CO3) was used in this study to produce controlled pores through the release of CO2 during the low-temperature decomposition of Na2CO3. Stage 3 focuses on 3D printing of binders using geopolymeric binders along with several OPC-based 3D printable binders. In Stage 4, synthesis and characterization of 3D-printable foamed fly ash-based geopolymer matrices for thermal insulation is the focus. A surfactant-based foaming process, multi-step mixing that ensures foam jamming transition and thus a dry foam, and microstructural packing to ensure adequate skeletal density are implemented to develop foamed suspensions amenable to 3D-printing. The last stage of this research develops 3D-printable alkali-activated ground granulated blast furnace slag mixture. Slag is used as the source of aluminosilicate and shows excellent mechanical properties when activated by highly alkaline activator (NaOH + sodium silicate solution). However, alkali activated slag sets and hardens rapidly which is undesirable for 3D printing. Thus, a novel mixing procedure is developed to significantly extend the setting time of slag activated with an alkaline activator to suit 3D printing applications without the use of any retarding admixtures. This dissertation, thus advances the field of sustainable and 3D-printable matrices and opens up a new avenue for faster and economical construction using specialized materials.
ContributorsAlghamdi, Hussam Suhail G (Author) / Neithalath, Narayanan (Thesis advisor) / Rajan, Subramaniam D. (Committee member) / Mobasher, Barzin (Committee member) / Abbaszadegan, Morteza (Committee member) / Bhate, Dhruv (Committee member) / Arizona State University (Publisher)
Created2019
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Description
Additive manufacturing, also known as 3-dimensional (3-d) printing, is now a rapidly growing manufacturing technique. Innovative and complex designs in various aspects of engineering have called for more efficient manufacturing techniques and 3-d printing has been a perfect choice in that direction. This research investigates the use of additive manufacturing

Additive manufacturing, also known as 3-dimensional (3-d) printing, is now a rapidly growing manufacturing technique. Innovative and complex designs in various aspects of engineering have called for more efficient manufacturing techniques and 3-d printing has been a perfect choice in that direction. This research investigates the use of additive manufacturing in fabricating polymer heat exchangers and estimate their effectiveness as a heat transfer device. Fused Deposition Modeling (FDM), Selective Laser Sintering (SLS) and Stereolithography (SLA) are the three 3-d printing techniques that are explored for their feasibility in manufacturing heat exchangers. The research also explores a triply periodic minimal structure–the gyroid, as a heat exchanger design. The performance of the gyroid heat exchanger was studied using experiments. The main parameters considered for the experiments were heat transfer rate, effectiveness and pressure drop. From the results obtained it can be inferred that using polymers in heat exchangers helps reducing corrosion and fouling problems, but it affects the effectiveness of the heat exchangers. For our design, the maximum effectiveness achieved was 0.1. The pressure drop for the heat exchanger was observed to decrease with an increase in flow rate and the maximum pressure drop measured was 0.88 psi for a flow rate of 5 LPM.
ContributorsDanayat, Swapneel Shailesh (Author) / Phelan, Patrick (Thesis advisor) / Kwon, Beomjin (Committee member) / Azeredo, Bruno (Committee member) / Arizona State University (Publisher)
Created2019
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Description
Traditionally, for applications that require heat transfer (e.g. heat exchangers),metals have been the go-to material for manufacturers because of their high thermal as
well as structural properties. However, metals have some notable drawbacks. They are
not corrosion-resistant, offer no freedom of design, have a high cost of production, and
sourcing the material itself.

Traditionally, for applications that require heat transfer (e.g. heat exchangers),metals have been the go-to material for manufacturers because of their high thermal as
well as structural properties. However, metals have some notable drawbacks. They are
not corrosion-resistant, offer no freedom of design, have a high cost of production, and
sourcing the material itself. Even though polymers on their own don’t show great
prospects in the field of thermal applications, their composites perform better than their
counterparts. Nanofillers, when added to a polymer matrix not only increase their
structural strength but also their thermal performance. This work aims to tackle two of
those problems by using the additive manufacturing method, stereolithography to solve
the problem of design freedom, and the use of polymer nanocomposite material for
corrosion-resistance and increase their overall thermal performance. In this work, three
different concentrations of polymer composite materials were studied: 0.25 wt%, 0.5
wt%, and 1wt% for their thermal conductivity. The samples were prepared by
magnetically stirring them for a period of 10 to 24 hours depending on their
concentrations and then sonicating in an ice bath further for a period of 2 to 3 hours.
These samples were then tested for their thermal conductivities using a Hot Disk TPS
2500S. Scanning Electron Microscope (SEM) to study the dispersion of the nanoparticles
in the matrix. Different theoretical models were studied and used to compare
experimental data to the predicted values of effective thermal conductivity. An increase
of 7.9 % in thermal conductivity of the composite material was recorded for just 1 wt%
addition of multiwalled carbon nanotubes (MWCNTs).
ContributorsGide, Kunal Manoj (Author) / Nian, Qiong (Thesis advisor) / Kwon, Beomjin (Committee member) / Li, Xiangjia (Committee member) / Arizona State University (Publisher)
Created2020