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The following is a report that will evaluate the microstructure of the nickel-based superalloy Hastelloy X and its relationship to mechanical properties in different load conditions. Hastelloy X is of interest to the company AORA because its strength and oxidation resistance at high temperatures is directly applicable to their needs

The following is a report that will evaluate the microstructure of the nickel-based superalloy Hastelloy X and its relationship to mechanical properties in different load conditions. Hastelloy X is of interest to the company AORA because its strength and oxidation resistance at high temperatures is directly applicable to their needs in a hybrid concentrated solar module. The literature review shows that the microstructure will produce different carbides at various temperatures, which can be beneficial to the strength of the alloy. These precipitates are found along the grain boundaries and act as pins that limit dislocation flow, as well as grain boundary sliding, and improve the rupture strength of the material. Over time, harmful precipitates form which counteract the strengthening effect of the carbides and reduce rupture strength, leading to failure. A combination of indentation and microstructure mapping was used in an effort to link local mechanical behavior to microstructure variability. Electron backscatter diffraction (EBSD) and energy dispersive spectroscopy (EDS) were initially used as a means to characterize the microstructure prior to testing. Then, a series of room temperature Vickers hardness tests at 50 and 500 gram-force were used to evaluate the variation in the local response as a function of indentation size. The room temperature study concluded that both the hardness and standard deviation increased at lower loads, which is consistent with the grain size distribution seen in the microstructure scan. The material was then subjected to high temperature spherical indentation. Load-displacement curves were essential in evaluating the decrease in strength of the material with increasing temperature. Through linear regression of the unloading portion of the curve, the plastic deformation was determined and compared at different temperatures as a qualitative method to evaluate local strength.
ContributorsCelaya, Andrew Jose (Author) / Peralta, Pedro (Thesis director) / Solanki, Kiran (Committee member) / Barrett, The Honors College (Contributor) / Mechanical and Aerospace Engineering Program (Contributor)
Created2015-05
Description
The study of the mechanical behavior of nanocrystalline metals using microelectromechanical systems (MEMS) devices lies at the intersection of nanotechnology, mechanical engineering and material science. The extremely small grains that make up nanocrystalline metals lead to higher strength but lower ductility as compared to bulk metals. Effects of strain-rate dependence

The study of the mechanical behavior of nanocrystalline metals using microelectromechanical systems (MEMS) devices lies at the intersection of nanotechnology, mechanical engineering and material science. The extremely small grains that make up nanocrystalline metals lead to higher strength but lower ductility as compared to bulk metals. Effects of strain-rate dependence on the mechanical behavior of nanocrystalline metals are explored. Knowing the strain rate dependence of mechanical properties would enable optimization of material selection for different applications and lead to lighter structural components and enhanced sustainability.
ContributorsHall, Andrea Paulette (Author) / Rajagopalan, Jagannathan (Thesis director) / Liao, Yabin (Committee member) / Barrett, The Honors College (Contributor) / Mechanical and Aerospace Engineering Program (Contributor)
Created2014-05
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Description
The goal of this research is to compare the mechanical properties of CP-Ti and Ti-O and to understand the relationship between a material's microstructure and its response to fatigue. Titanium has been selected due to its desirable properties and applicability in several engineering fields. Both samples are polished and etched

The goal of this research is to compare the mechanical properties of CP-Ti and Ti-O and to understand the relationship between a material's microstructure and its response to fatigue. Titanium has been selected due to its desirable properties and applicability in several engineering fields. Both samples are polished and etched in order to visualize and characterize the microstructure and its features. The samples then undergo strain-controlled fatigue tests for several thousand cycles. Throughout testing, images of the samples are taken at zero and maximum load for DIC analysis. The DIC results can be used to study the local strains of the samples. The DIC analysis performed on the CP-Ti sample and presented in this study will be used to understand how the addition of oxygen in the Ti-O impacts fatigue response. The outcome of this research can be used to develop long-lasting, high strength materials.
ContributorsRiley, Erin Ashland (Author) / Solanki, Kiran (Thesis director) / Oswald, Jay (Committee member) / School of Art (Contributor) / Mechanical and Aerospace Engineering Program (Contributor) / Barrett, The Honors College (Contributor)
Created2016-05
Description

This study experimentally investigated a selected methodology of mechanical torque testing of 3D printed gears. The motivation for pursuing this topic of research stemmed from a previous experience of one of the team members that propelled inspiration to quantify how different variables associated with 3D printing affect the structural integrity

This study experimentally investigated a selected methodology of mechanical torque testing of 3D printed gears. The motivation for pursuing this topic of research stemmed from a previous experience of one of the team members that propelled inspiration to quantify how different variables associated with 3D printing affect the structural integrity of the resulting piece. With this goal in mind, the team set forward with creating an experimental set-up and the construction of a test rig. However, due to restrictions in time and other unforeseen circumstances, this thesis underwent a change in scope. The new scope focused solely on determining if the selected methodology of mechanical torque testing was valid. Following the securement of parts and construction of a test rig, the team was able to conduct mechanical testing. This testing was done multiple times on an identically printed gear. The data collected showed results similar to a stress-strain curve when the torque was plotted against the angle of twist. In the resulting graph, the point of plastic deformation is clearly visible and the maximum torque the gear could withstand is clearly identifiable. Additionally, across the tests conducted, the results show high similarity in results. From this, it is possible to conclude that if the tests were repeated multiple times the maximum possible torque could be found. From that maximum possible torque, the mechanical strength of the tested gear could be identified.

ContributorsGarcia, Andres (Author) / Parekh, Mohan (Co-author) / Middleton, James (Thesis director) / Murthy, Raghavendra (Committee member) / Barrett, The Honors College (Contributor) / Mechanical and Aerospace Engineering Program (Contributor)
Created2023-05
Description

This study experimentally investigated a selected methodology of mechanical torque testing of 3D printed gears. The motivation for pursuing this topic of research stemmed from a previous experience of one of the team members that propelled inspiration to quantify how different variables associated with 3D printing affect the structural integrity

This study experimentally investigated a selected methodology of mechanical torque testing of 3D printed gears. The motivation for pursuing this topic of research stemmed from a previous experience of one of the team members that propelled inspiration to quantify how different variables associated with 3D printing affect the structural integrity of the resulting piece. With this goal in mind, the team set forward with creating an experimental set-up and the construction of a test rig. However, due to restrictions in time and other unforeseen circumstances, this thesis underwent a change in scope. The new scope focused solely on determining if the selected methodology of mechanical torque testing was valid. Following the securement of parts and construction of a test rig, the team was able to conduct mechanical testing. This testing was done multiple times on an identically printed gear. The data collected showed results similar to a stress-strain curve when the torque was plotted against the angle of twist. In the resulting graph, the point of plastic deformation is clearly visible and the maximum torque the gear could withstand is clearly identifiable. Additionally, across the tests conducted, the results show high similarity in results. From this, it is possible to conclude that if the tests were repeated multiple times the maximum possible torque could be found. From that maximum possible torque, the mechanical strength of the tested gear could be identified.

ContributorsParekh, Mohan (Author) / Garcia, Andres (Co-author) / Middleton, James (Thesis director) / Murthy, Raghavendra (Committee member) / Barrett, The Honors College (Contributor) / Mechanical and Aerospace Engineering Program (Contributor)
Created2023-05
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Description
This paper investigates Surface Mechanical Attrition Treatment (SMAT) and the influence of treatment temperature and initial sample surface finish on the corrosion resistance of 7075-T651 aluminum alloy. Ambient SMAT was performed on AA7075 samples polished to 80-grit initial surface roughness. Potentiodynamic polarization and electrochemical impedance spectroscopy (EIS) tests were used

This paper investigates Surface Mechanical Attrition Treatment (SMAT) and the influence of treatment temperature and initial sample surface finish on the corrosion resistance of 7075-T651 aluminum alloy. Ambient SMAT was performed on AA7075 samples polished to 80-grit initial surface roughness. Potentiodynamic polarization and electrochemical impedance spectroscopy (EIS) tests were used to characterize the corrosion behavior of samples before and after SMAT. Electrochemical tests indicated an improved corrosion resistance after application of SMAT process. The observed improvements in corrosion properties are potentially due to microstructural changes in the material surface induced by SMAT which encouraged the formation of a passive oxide layer. Further testing and research are required to understand the corrosion related effects of cryogenic SMAT and initial-surface finish as the COVID-19 pandemic inhibited experimentation plans.
ContributorsDeorio, Jordan Anthony (Author) / Solanki, Kiran (Thesis director) / Rajagopalan, Jagannathan (Committee member) / Mechanical and Aerospace Engineering Program (Contributor) / Barrett, The Honors College (Contributor)
Created2020-05