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Description
Soft magnetic alloys play a significant role for magnetic recording applications and highly sensitivity magnetic field sensors. In order to sustain the magnetic areal density growth, development of new synthesis techniques and materials is necessary. In this work, the effect of oxygen incorporation during electrodeposition of CoFe alloys on magnetic properties, magnetoresistance and structural properties has been studied. Understanding the magnetic properties often required knowledge of oxygen distribution and structural properties of the grown films. Transmission electron microscopy (TEM) was a powerful tool in this study to correlate the oxygen-distribution nanostructure to the magnetic properties of deposited films. Off-axis electron holography in TEM was used to measure magnetic domain wall width in the deposited films. Elemental depth profiles of Fe, Co, O were investigated by secondary ion mass spectroscopy (SIMS). Magnetic properties have been determined by superconducting quantum interference device (SQUID) measurements. Oxygen content in the CoFe deposited films was controlled by electrolyte composition. Films were deposited on Si 100 substrates and on other substrates such as Cu and Al. However, a good film quality was achieved on Si substrate. Electron energy loss and x-ray spectroscopies showed that the low oxygen films contained intragranular Fe2+ oxide (FeO) particles and that the high oxygen films contained intergranular Fe3+ (Fe2O3) along grain boundaries. The films with oxide present at the grain boundary had significantly increased coercivity, magnetoresistance and reduced saturation magnetization relative to the lower oxygen content films with intragranular oxide. The differences in magnetic properties between low oxygen and high oxygen concentration films were attributed to stronger mobile domain wall interactions with the grain boundary oxide layers. The very high magnetoresistance values were achieved for magnetic devices with nanocontact dimension < 100 nm and oxide incorporation in this nanoconfined geometry. The content of oxide phase in nanocontact was controlled by concentration of the Fe3+ ions in the electrodeposition solution. Magnetic device integrity was improved by varying amount of additive into plating solution. These results indicated that electrodeposited CoFe nanocontact is a novel class of materials with large application for magnetic field sensors.
ContributorsElhalawaty, Shereen (Author) / Carpenter, Ray (Thesis advisor) / Chamberlin, Ralph (Committee member) / McCartney, Martha (Committee member) / Alford, Terry (Committee member) / Arizona State University (Publisher)
Created2012
Description
A system for illuminating a sample in situ with visible and UV light inside a transmission electron microscope was devised to study photocatalysts. There are many factors which must be considered when designing and building such a system. These include both mechanical, optical, and electron optical considerations. Some of the restrictions posed by the electron microscope column are significant, and care must be taken not to degrade the microscope's electron optical performance, or to unduly restrict the other current capabilities of the microscope. The nature of these various design considerations is discussed in detail. A description of the system that has been added to the microscope at ASU, an FEI Tecnai F20 environmental transmission electron microscope is also given. The system includes a high brightness broadband light source with optical filters, a fiber to guide the light to the sample, and a system for precisely aligning the fiber tip. The spatial distribution and spectrum of the light reaching the sample has been characterized, and is described in detail.
ContributorsMiller, Benjamin (Author) / Crozier, Peter A. (Thesis advisor) / McCartney, Martha (Committee member) / Rez, Peter (Committee member) / Arizona State University (Publisher)
Created2012
Description
This thesis encompasses research performed in the focus area of structural health monitoring. More specifically, this research focuses on high velocity impact testing of carbon fiber reinforced structures, especially plates, and evaluating the damage post-impact. To this end, various non-destructive evaluation techniques such as ultrasonic C-scan testing and flash thermography were utilized for post-impact analysis. MATLAB algorithms were written and refined for the localization and quantification of damage in plates using data from sensors such as piezoelectric and fiber Bragg gratings sensors. Throughout the thesis, the general plate theory and laminate plate theory, the operations and optimization of the gas gun, and the theory used for the damage localization algorithms will be discussed. Additional quantifiable results are to come in future semesters of experimentation, but this thesis outlines the framework upon which all the research will continue to advance.
ContributorsMccrea, John Patrick (Author) / Chattopadhyay, Aditi (Thesis director) / Borkowski, Luke (Committee member) / Barrett, The Honors College (Contributor) / Mechanical and Aerospace Engineering Program (Contributor) / Department of Military Science (Contributor)
Created2015-05
Description
This paper describes the research done to attempt to scale up thrusts produced by ionic wind thrusters, or "lifters" to magnitudes needed to power a 2 kg hobbyist remote-control airplane. It includes background information on the Biefeld-Brown effect and the thrust it produces, an experiment that attempted to prove that thrust can be scaled up from smaller ionic wind thrusters to larger scales, and two models predicting thruster geometries and power sources needed to reach these thrusts. An ionic wind thruster could not be created that would power the hobbyist remote as a high-voltage power source with voltage and power high enough could not be obtained. Thrusters were created for the experiment using balsa wood, aluminum foil, and thin copper wire, and were powered using a 30 kV transformer. The thrusters attempted to test for correlations between thrust, electrode length, and current; electric field strength, and thrust; and thrust optimization through opening up air flow through the collector electrode. The experiment was inconclusive as all the thrusters failed to produce measurable thrust. Further experimentation suggests the chief failure mode is likely conduction from the collector electrode to the nearby large conductive surface of the scale.
ContributorsHaug, Andrew James (Author) / White, Daniel (Thesis director) / Takahashi, Timothy (Committee member) / Middleton, James (Committee member) / Mechanical and Aerospace Engineering Program (Contributor) / Department of Military Science (Contributor) / Barrett, The Honors College (Contributor)
Created2017-12