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Description
In the nano-regime many materials exhibit properties that are quite different from their bulk counterparts. These nano-properties have been shown to be useful in a wide range of applications with nanomaterials being used for catalysts, in energy production, as protective coatings, and in medical treatment. While there is no shortage

In the nano-regime many materials exhibit properties that are quite different from their bulk counterparts. These nano-properties have been shown to be useful in a wide range of applications with nanomaterials being used for catalysts, in energy production, as protective coatings, and in medical treatment. While there is no shortage of exciting and novel applications, the world of nanomaterials suffers from a lack of large scale manufacturing techniques. The current methods and equipment used for manufacturing nanomaterials are generally slow, expensive, potentially dangerous, and material specific. The research and widespread use of nanomaterials has undoubtedly been hindered by this lack of appropriate tooling. This work details the effort to create a novel nanomaterial synthesis and deposition platform capable of operating at industrial level rates and reliability.

The tool, referred to as Deppy, deposits material via hypersonic impaction, a two chamber process that takes advantage of compressible fluids operating in the choked flow regime to accelerate particles to up several thousand meters per second before they impact and stick to the substrate. This allows for the energetic separation of the synthesis and deposition processes while still behaving as a continuous flow reactor giving Deppy the unique ability to independently control the particle properties and the deposited film properties. While the ultimate goal is to design a tool capable of producing a broad range of nanomaterial films, this work will showcase Deppy's ability to produce silicon nano-particle films as a proof of concept.

By adjusting parameters in the upstream chamber the particle composition was varied from completely amorphous to highly crystalline as confirmed by Raman spectroscopy. By adjusting parameters in the downstream chamber significant variation of the film's density was achieved. Further it was shown that the system is capable of making these adjustments in each chamber without affecting the operation of the other.
ContributorsFirth, Peter (Author) / Holman, Zachary C (Thesis advisor) / Kozicki, Michael (Committee member) / Goryll, Michael (Committee member) / Arizona State University (Publisher)
Created2015
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Description
Nanomaterials exhibit unique properties that are substantially different from their bulk counterparts. These unique properties have gained recognition and application for various fields and products including sensors, displays, photovoltaics, and energy storage devices. Aerosol Deposition (AD) is a relatively new method for depositing nanomaterials. AD utilizes a nozzle to accelerate

Nanomaterials exhibit unique properties that are substantially different from their bulk counterparts. These unique properties have gained recognition and application for various fields and products including sensors, displays, photovoltaics, and energy storage devices. Aerosol Deposition (AD) is a relatively new method for depositing nanomaterials. AD utilizes a nozzle to accelerate the nanomaterial into a deposition chamber under near-vacuum conditions towards a substrate with which the nanomaterial collides and adheres. Traditional methods for designing nozzles at atmospheric conditions are not well suited for nozzle design for AD methods.

Computational Fluid Dynamics (CFD) software, ANSYS Fluent, is utilized to simulate two-phase flows consisting of a carrier gas (Helium) and silicon nanoparticles. The Cunningham Correction Factor is used to account for non-continuous effects at the relatively low pressures utilized in AD.

The nozzle, referred to herein as a boundary layer compensation (BLC) nozzle, comprises an area-ratio which is larger than traditionally designed nozzles to compensate for the thick boundary layer which forms within the viscosity-affected carrier gas flow. As a result, nanoparticles impact the substrate at velocities up to 300 times faster than the baseline nozzle.
ContributorsHoffman, Trent (Author) / Holman, Zachary C (Thesis advisor) / Herrmann, Marcus (Committee member) / Kozicki, Michael (Committee member) / Arizona State University (Publisher)
Created2017
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Description
The Built-In Self-Test for Simultaneous Transmit and Receive (BIST for STAR) will be able to solve the challenges of transmitting and receiving at the same time at the same frequency. One of the major components is the STAR antenna which transmits and receives along the same pathway. The main problem

The Built-In Self-Test for Simultaneous Transmit and Receive (BIST for STAR) will be able to solve the challenges of transmitting and receiving at the same time at the same frequency. One of the major components is the STAR antenna which transmits and receives along the same pathway. The main problem with doing both on the same path is that the transmit signal is usually much stronger in power compared to the received signal. The transmit signal has echoes and leakages that cause self-interference, preventing the received signal from being properly obtained. The solution developed in this project is the BIST component, which will help calculate the functional gain and phase offset of the interference signal and subtract it from the pathway so that the received signal remains. The functions of the proposed circuit board can be modeled in Matlab, where an emulation code generates a random, realistic functional gain and delay for the interference. From the generated values, the BIST for STAR was simulated to output what the measurements would be given the strength of the input signal and a controlled delay. The original Matlab code models an ideal environment directly recalculating the functional gain and phase from the given measurements in a second Matlab script. The actual product will not be ideal; a possible source of error to be considered is the effect of thermal noise. To observe the effect of noise on the BIST for STAR's performance, the Matlab code was expanded upon to include a component for thermal noise, and a method of analyzing the results of the board.
ContributorsLiu, Jennifer Yuan (Author) / Ozev, Sule (Thesis director) / Kozicki, Michael (Committee member) / Electrical Engineering Program (Contributor) / Barrett, The Honors College (Contributor)
Created2016-05
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Description
The capstone portion of this project was to use the established STaR antennas and add a Built in Self-Test system to ensure the quality of the signals being received. This part of the project required a MatLab simulation to be built, a layout created, and a PCB designed for fabrication.

The capstone portion of this project was to use the established STaR antennas and add a Built in Self-Test system to ensure the quality of the signals being received. This part of the project required a MatLab simulation to be built, a layout created, and a PCB designed for fabrication. In theory, the test BiST unit will allow the gain and delay of the transmitted signal and then cancel out unneeded interference for the received signal. However, this design required multiple paths to maintain the same lengths to keep the signals in phase for comparison. The purpose of this thesis is to show the potential drop-offs of the quality of the signals from being out of phase due to the wires that should be similar, being off by a certain percentage. This project will calculate the theoretical delay of all wires being out of sync and then add this delay to the established MatLab simulation. This report will show the relationship between the error of the received variables and what the actual generated values. And, the last part of the document will demonstrate the simulation by creating a signal and comparing it to its received counterpart. The end result of the study showed that the percent error between what is seen and what is expected is near insignificant and, hence, not an issue with regards to the quality of the project.
ContributorsSomers, Tyler Scott (Author) / Ozev, Sule (Thesis director) / Kozicki, Michael (Committee member) / Electrical Engineering Program (Contributor) / Barrett, The Honors College (Contributor)
Created2016-05
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Description
The purpose of the Simultaneous Transmit and Receive Antenna project is to design a test circuit that will allow us to use an antenna to both send out and receive a signal at the same time on the same frequency. The test circuit will generate DC voltage levels that we

The purpose of the Simultaneous Transmit and Receive Antenna project is to design a test circuit that will allow us to use an antenna to both send out and receive a signal at the same time on the same frequency. The test circuit will generate DC voltage levels that we can use to solve for the gain and delay of the transmit interference, so we will then be able to cancel out the unwanted signal from the received signal. With a theoretically perfect setup, the transmitted signal will be able to be completely isolated from the received signal, leaving us with only what we want at the output. In practice, however, this is not the case. There are many variables that will affect the integrity of the DC output of the test signal. As the output voltage level deviates from its theoretical perfect measurement, the precision to which we are able to solve for the gain and delay values decreases. The focus of this study is to estimate the effect of using a digital measurement tool to measure the output of the test circuit. Assuming a voltmeter with 1 volt full range, simulations were run using measurements stored at different bit resolutions, from 8-bit storage up to 16-bit storage. Since the physical hardware for the Simultaneous Transmit and Receive test circuit is not currently available, these tests were performed with an edited version of the Matlab simulation created for the Senior Design project. The simulation was run 2000 times over each bit resolution to get a wide range of generated values, then the error from each run was analyzed to come to a conclusion on the effect of the digital measurement on the design. The results of these simulations as well as further details of the project and testing are described inside this document.
ContributorsKral, Brandon Michael (Author) / Ozev, Sule (Thesis director) / Kozicki, Michael (Committee member) / Electrical Engineering Program (Contributor) / Barrett, The Honors College (Contributor)
Created2016-05