Theses and Dissertations
This collection includes both ASU Theses and Dissertations, submitted by graduate students, and the Barrett, Honors College theses submitted by undergraduate students.
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- Creators: Li, Hechao
- Creators: Turaga, Pavan
Description
An accurate knowledge of the complex microstructure of a heterogeneous material is crucial for quantitative structure-property relations establishment and its performance prediction and optimization. X-ray tomography has provided a non-destructive means for microstructure characterization in both 3D and 4D (i.e., structural evolution over time). Traditional reconstruction algorithms like filtered-back-projection (FBP) method or algebraic reconstruction techniques (ART) require huge number of tomographic projections and segmentation process before conducting microstructural quantification. This can be quite time consuming and computationally intensive.
In this thesis, a novel procedure is first presented that allows one to directly extract key structural information in forms of spatial correlation functions from limited x-ray tomography data. The key component of the procedure is the computation of a “probability map”, which provides the probability of an arbitrary point in the material system belonging to specific phase. The correlation functions of interest are then readily computed from the probability map. Using effective medium theory, accurate predictions of physical properties (e.g., elastic moduli) can be obtained.
Secondly, a stochastic optimization procedure that enables one to accurately reconstruct material microstructure from a small number of x-ray tomographic projections (e.g., 20 - 40) is presented. Moreover, a stochastic procedure for multi-modal data fusion is proposed, where both X-ray projections and correlation functions computed from limited 2D optical images are fused to accurately reconstruct complex heterogeneous materials in 3D. This multi-modal reconstruction algorithm is proved to be able to integrate the complementary data to perform an excellent optimization procedure, which indicates its high efficiency in using limited structural information.
Finally, the accuracy of the stochastic reconstruction procedure using limited X-ray projection data is ascertained by analyzing the microstructural degeneracy and the roughness of energy landscape associated with different number of projections. Ground-state degeneracy of a microstructure is found to decrease with increasing number of projections, which indicates a higher probability that the reconstructed configurations match the actual microstructure. The roughness of energy landscape can also provide information about the complexity and convergence behavior of the reconstruction for given microstructures and projection number.
In this thesis, a novel procedure is first presented that allows one to directly extract key structural information in forms of spatial correlation functions from limited x-ray tomography data. The key component of the procedure is the computation of a “probability map”, which provides the probability of an arbitrary point in the material system belonging to specific phase. The correlation functions of interest are then readily computed from the probability map. Using effective medium theory, accurate predictions of physical properties (e.g., elastic moduli) can be obtained.
Secondly, a stochastic optimization procedure that enables one to accurately reconstruct material microstructure from a small number of x-ray tomographic projections (e.g., 20 - 40) is presented. Moreover, a stochastic procedure for multi-modal data fusion is proposed, where both X-ray projections and correlation functions computed from limited 2D optical images are fused to accurately reconstruct complex heterogeneous materials in 3D. This multi-modal reconstruction algorithm is proved to be able to integrate the complementary data to perform an excellent optimization procedure, which indicates its high efficiency in using limited structural information.
Finally, the accuracy of the stochastic reconstruction procedure using limited X-ray projection data is ascertained by analyzing the microstructural degeneracy and the roughness of energy landscape associated with different number of projections. Ground-state degeneracy of a microstructure is found to decrease with increasing number of projections, which indicates a higher probability that the reconstructed configurations match the actual microstructure. The roughness of energy landscape can also provide information about the complexity and convergence behavior of the reconstruction for given microstructures and projection number.
ContributorsLi, Hechao (Author) / Jiao, Yang (Thesis advisor) / Chawla, Nikhilesh (Committee member) / Liu, Yongming (Committee member) / Ren, Yi (Committee member) / Mu, Bin (Committee member) / Arizona State University (Publisher)
Created2017
Description
Semantic image segmentation has been a key topic in applications involving image processing and computer vision. Owing to the success and continuous research in the field of deep learning, there have been plenty of deep learning-based segmentation architectures that have been designed for various tasks. In this thesis, deep-learning architectures for a specific application in material science; namely the segmentation process for the non-destructive study of the microstructure of Aluminum Alloy AA 7075 have been developed. This process requires the use of various imaging tools and methodologies to obtain the ground-truth information. The image dataset obtained using Transmission X-ray microscopy (TXM) consists of raw 2D image specimens captured from the projections at every beam scan. The segmented 2D ground-truth images are obtained by applying reconstruction and filtering algorithms before using a scientific visualization tool for segmentation. These images represent the corrosive behavior caused by the precipitates and inclusions particles on the Aluminum AA 7075 alloy. The study of the tools that work best for X-ray microscopy-based imaging is still in its early stages.
In this thesis, the underlying concepts behind Convolutional Neural Networks (CNNs) and state-of-the-art Semantic Segmentation architectures have been discussed in detail. The data generation and pre-processing process applied to the AA 7075 Data have also been described, along with the experimentation methodologies performed on the baseline and four other state-of-the-art Segmentation architectures that predict the segmented boundaries from the raw 2D images. A performance analysis based on various factors to decide the best techniques and tools to apply Semantic image segmentation for X-ray microscopy-based imaging was also conducted.
In this thesis, the underlying concepts behind Convolutional Neural Networks (CNNs) and state-of-the-art Semantic Segmentation architectures have been discussed in detail. The data generation and pre-processing process applied to the AA 7075 Data have also been described, along with the experimentation methodologies performed on the baseline and four other state-of-the-art Segmentation architectures that predict the segmented boundaries from the raw 2D images. A performance analysis based on various factors to decide the best techniques and tools to apply Semantic image segmentation for X-ray microscopy-based imaging was also conducted.
ContributorsBarboza, Daniel (Author) / Turaga, Pavan (Thesis advisor) / Chawla, Nikhilesh (Committee member) / Jayasuriya, Suren (Committee member) / Arizona State University (Publisher)
Created2020