Matching Items (3)
Filtering by
- All Subjects: Atomic Force Microscopy
- Creators: Yekani Fard, Masoud
- Creators: Baker, Dylan Paul
Description
This thesis document outlines the construction of a device for preparation of cylindrical ice-aluminum specimens. These specimens are for testing in a uniaxial load cell with the goal of determining properties of the ice-metal interface, as part of research into spray ice material properties and how such ice might be better removed from maritime vessels operating in sub-freezing temperatures. The design of the sample preparation device is outlined, justifications for design and component choices given and discussion of the design process and how problems which arose were tackled are included. Water is piped into the device through the freezers lid and sprayed by a full cone misting nozzle onto an aluminum sample rod. The sample rod is supported with Ultra High Molecular Weight Polyethylene pillars which allow for free rotation. A motor, timing belt and pulley assembly is used to rotate this metal rod at 1.25 RPM. The final device produces samples though intermittent flow in a 5 minutes on, 20 minutes off cycle. This intermittent flow is controlled through the use of a solenoid valve which is wired into the compressor. When the thermostat detects that the freezer is too warm, the compressor kicks on and the flow of water is stopped. Additional modifications to the freezer unit include the addition of a fan to cool the compressor during device operation. Recommendations are provided towards the end of the thesis, including suggestions to change the device to allow for constant flow and that deionized water be used instead of tap water due to hard water concerns.
ContributorsBaker, Dylan Paul (Author) / Oswald, Jay (Thesis director) / Yekani Fard, Masoud (Committee member) / Mechanical and Aerospace Engineering Program (Contributor) / Barrett, The Honors College (Contributor)
Created2016-12
Description
Carbon Fiber Reinforced Polymers (CFRP) are a promising engineering material because of their multifunctionality and desirable mechanical, electrical, and thermal properties. The mechanical and fracture properties of CFRPs rely on effective stress transfer from the bulk matrix to individual carbon fibers. Pristine carbon fibers (CF) are chemically unreactive and smooth, which inhibits stress transfer mechanisms and makes CF susceptible to matrix debonding. Current composite research aims to improve the synergy between the CF and surrounding matrix by engineering the interphase. The composite interphase is characterized by mechanical properties deviating from the fiber and matrix properties. Carbon nanotubes (CNT), graphene nanoplatelets, and other carbon nanofillers have been studied extensively for their interphase-enhancing capabilities.
ContributorsPensky, Alek R (Author) / Yekani Fard, Masoud (Thesis director) / Zhu, Haolin (Committee member) / Mechanical and Aerospace Engineering Program (Contributor) / Barrett, The Honors College (Contributor)
Created2020-05
Description
This experiment analyzed the degradation mechanisms in polymer matrix composite (PMC) samples after more than 50 years of simulated exposure to hygrothermal conditioning. This strong, form-adaptive, lightweight material is suitable for use on critical structures including nuclear powerplants and spacecrafts as primary reinforcers to improve fracture toughness. Current literature regarding PMC material has a poor understanding of its delamination trends and varying interphase properties that determine its overall reliability under extreme weather conditions. This paper will evaluate the long-term impact from exposure to heat and humidity regarding the material’s stiffness and degradation to confirm PMC’s reliability for use in structures that undergo these conditions. To study this phenomenon, aged and unaged PMC samples were analyzed on the nanoscale using PeakForce Quantitative Nanomechanical mode (PF-QNM) of Atomic Force Microscopy with an indentation tip no greater than 10nm in radius. This paper compares this testing method to the results from recent research on other microscopy modes to discuss the validity of the PF-QNM model as it is used for this analysis. The data obtained allowed for analysis of crack propagation and quantification of strength in interphase between the composite’s constituents. This research verifies the testing method for which a comprehensive understanding of the environmental influences on PMC mechanical properties could be achieved.
ContributorsTotillo, Anita (Co-author, Co-author) / Yekani Fard, Masoud (Thesis director) / Patel, Jay (Committee member) / Mechanical and Aerospace Engineering Program (Contributor) / Barrett, The Honors College (Contributor)
Created2019-05