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Description
Recently, the use of zinc oxide (ZnO) nanowires as an interphase in composite materials has been demonstrated to increase the interfacial shear strength between carbon fiber and an epoxy matrix. In this research work, the strong adhesion between ZnO and carbon fiber is investigated to elucidate the interactions at the

Recently, the use of zinc oxide (ZnO) nanowires as an interphase in composite materials has been demonstrated to increase the interfacial shear strength between carbon fiber and an epoxy matrix. In this research work, the strong adhesion between ZnO and carbon fiber is investigated to elucidate the interactions at the interface that result in high interfacial strength. First, molecular dynamics (MD) simulations are performed to calculate the adhesive energy between bare carbon and ZnO. Since the carbon fiber surface has oxygen functional groups, these were modeled and MD simulations showed the preference of ketones to strongly interact with ZnO, however, this was not observed in the case of hydroxyls and carboxylic acid. It was also found that the ketone molecules ability to change orientation facilitated the interactions with the ZnO surface. Experimentally, the atomic force microscope (AFM) was used to measure the adhesive energy between ZnO and carbon through a liftoff test by employing highly oriented pyrolytic graphite (HOPG) substrate and a ZnO covered AFM tip. Oxygen functionalization of the HOPG surface shows the increase of adhesive energy. Additionally, the surface of ZnO was modified to hold a negative charge, which demonstrated an increase in the adhesive energy. This increase in adhesion resulted from increased induction forces given the relatively high polarizability of HOPG and the preservation of the charge on ZnO surface. It was found that the additional negative charge can be preserved on the ZnO surface because there is an energy barrier since carbon and ZnO form a Schottky contact. Other materials with the same ionic properties of ZnO but with higher polarizability also demonstrated good adhesion to carbon. This result substantiates that their induced interaction can be facilitated not only by the polarizability of carbon but by any of the materials at the interface. The versatility to modify the magnitude of the induced interaction between carbon and an ionic material provides a new route to create interfaces with controlled interfacial strength.
ContributorsGalan Vera, Magdian Ulises (Author) / Sodano, Henry A (Thesis advisor) / Jiang, Hanqing (Committee member) / Solanki, Kiran (Committee member) / Oswald, Jay (Committee member) / Speyer, Gil (Committee member) / Arizona State University (Publisher)
Created2013
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Description
Ingestion of high temperature mainstream gas into the rotor-stator cavities of a gas turbine is one of the major problems faced by the turbine designers. The ingested gas heats up rotor disks and induces higher thermal stresses on them, giving rise to durability concern. Ingestion is usually reduced by installing

Ingestion of high temperature mainstream gas into the rotor-stator cavities of a gas turbine is one of the major problems faced by the turbine designers. The ingested gas heats up rotor disks and induces higher thermal stresses on them, giving rise to durability concern. Ingestion is usually reduced by installing seals on the rotor and stator rims and by purging the disk cavity by secondary air bled from the compressor discharge. The geometry of the rim seals and the secondary air flow rate, together, influence the amount of gas that gets ingested into the cavities. Since the amount of secondary air bled off has a negative effect on the gas turbine thermal efficiency, one goal is to use the least possible amount of secondary air. This requires a good understanding of the flow and ingestion fields within a disk cavity. In the present study, the mainstream gas ingestion phenomenon has been experimentally studied in a model single-stage axial flow gas turbine. The turbine stage featured vanes and blades, and rim seals on both the rotor and stator. Additionally, the disk cavity contained a labyrinth seal radially inboard which effectively divided the cavity into a rim cavity and an inner cavity. Time-average static pressure measurements were obtained at various radial positions within the disk cavity, and in the mainstream gas path at three axial locations at the outer shroud spread circumferentially over two vane pitches. The time-average static pressure in the main gas path exhibited a periodic asymmetry following the vane pitch whose amplitude diminished with increasing distance from the vane trailing edge. The static pressure distribution increased with the secondary air flow rate within the inner cavity but was found to be almost independent of it in the rim cavity. Tracer gas (CO2) concentration measurements were conducted to determine the sealing effectiveness of the rim seals against main gas ingestion. For the rim cavity, the sealing effectiveness increased with the secondary air flow rate. Within the inner cavity however, this trend reversed -this may have been due to the presence of rotating low-pressure flow structures inboard of the labyrinth seal.
ContributorsThiagarajan, Jayanth kumar (Author) / Roy, Ramendra P (Thesis advisor) / Lee, Taewoo (Committee member) / Mignolet, Marc (Committee member) / Arizona State University (Publisher)
Created2013
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Description
Shock loading is a complex phenomenon that can lead to failure mechanisms such as strain localization, void nucleation and growth, and eventually spall fracture. Studying incipient stages of spall damage is of paramount importance to accurately determine initiation sites in the material microstructure where damage will nucleate and grow and

Shock loading is a complex phenomenon that can lead to failure mechanisms such as strain localization, void nucleation and growth, and eventually spall fracture. Studying incipient stages of spall damage is of paramount importance to accurately determine initiation sites in the material microstructure where damage will nucleate and grow and to formulate continuum models that account for the variability of the damage process due to microstructural heterogeneity. The length scale of damage with respect to that of the surrounding microstructure has proven to be a key aspect in determining sites of failure initiation. Correlations have been found between the damage sites and the surrounding microstructure to determine the preferred sites of spall damage, since it tends to localize at and around the regions of intrinsic defects such as grain boundaries and triple points. However, considerable amount of work still has to be done in this regard to determine the physics driving the damage at these intrinsic weak sites in the microstructure. The main focus of this research work is to understand the physical mechanisms behind the damage localization at these preferred sites. A crystal plasticity constitutive model is implemented with different damage criteria to study the effects of stress concentration and strain localization at the grain boundaries. A cohesive zone modeling technique is used to include the intrinsic strength of the grain boundaries in the simulations. The constitutive model is verified using single elements tests, calibrated using single crystal impact experiments and validated using bicrystal and multicrystal impact experiments. The results indicate that strain localization is the predominant driving force for damage initiation and evolution. The microstructural effects on theses damage sites are studied to attribute the extent of damage to microstructural features such as grain orientation, misorientation, Taylor factor and the grain boundary planes. The finite element simulations show good correlation with the experimental results and can be used as the preliminary step in developing accurate probabilistic models for damage nucleation.
ContributorsKrishnan, Kapil (Author) / Peralta, Pedro (Thesis advisor) / Mignolet, Marc (Committee member) / Sieradzki, Karl (Committee member) / Jiang, Hanqing (Committee member) / Oswald, Jay (Committee member) / Arizona State University (Publisher)
Created2013
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Description
As robots are increasingly migrating out of factories and research laboratories and into our everyday lives, they should move and act in environments designed for humans. For this reason, the need of anthropomorphic movements is of utmost importance. The objective of this thesis is to solve the inverse kinematics problem

As robots are increasingly migrating out of factories and research laboratories and into our everyday lives, they should move and act in environments designed for humans. For this reason, the need of anthropomorphic movements is of utmost importance. The objective of this thesis is to solve the inverse kinematics problem of redundant robot arms that results to anthropomorphic configurations. The swivel angle of the elbow was used as a human arm motion parameter for the robot arm to mimic. The swivel angle is defined as the rotation angle of the plane defined by the upper and lower arm around a virtual axis that connects the shoulder and wrist joints. Using kinematic data recorded from human subjects during every-day life tasks, the linear sensorimotor transformation model was validated and used to estimate the swivel angle, given the desired end-effector position. Defining the desired swivel angle simplifies the kinematic redundancy of the robot arm. The proposed method was tested with an anthropomorphic redundant robot arm and the computed motion profiles were compared to the ones of the human subjects. This thesis shows that the method computes anthropomorphic configurations for the robot arm, even if the robot arm has different link lengths than the human arm and starts its motion at random configurations.
ContributorsWang, Yuting (Author) / Artemiadis, Panagiotis (Thesis advisor) / Mignolet, Marc (Committee member) / Santos, Veronica J (Committee member) / Arizona State University (Publisher)
Created2013
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Description
Cavitation erosion is a significant cause of wear in marine components, such as impellers, propellers or rudders. While the erosion process has been widely studied on metals, the effect of cavitation on polymers is not well-understood. The stress response in metals differs greatly from that of polymers, e.g. rate and

Cavitation erosion is a significant cause of wear in marine components, such as impellers, propellers or rudders. While the erosion process has been widely studied on metals, the effect of cavitation on polymers is not well-understood. The stress response in metals differs greatly from that of polymers, e.g. rate and temperature effects are far more important, thus damage and wear mechanisms of polymers under cavitating flows are significantly different. In this work, heat-driven failure caused by viscous dissipation and void nucleation resulting from tensile stresses arising from stress wave reflections are investigated as two possible material failure mechanisms.

As a first step in developing a fundamental understanding of the cavitation erosion process on polymer surfaces, simulations are performed of the collapse of individual bubbles against a compliant surface e.g. metallic substrates with polyurea coatings. The surface response of collapse-driven impact loads is represented by a idealized, time-dependent, Gaussian pressure distribution on the surface. A two-dimensional distribution of load radii and durations is considered corresponding to characteristic of cavitating flows accelerated erosion experiments. Finite element simulations are performed to fit a response curve that relates the loading parameters to the energy dissipated in the coating and integrated with collapse statistics to generate an expected heat input into the coating.

The impulsive pressure, which is generated due to bubble collapse, impacts the material and generates intense shock waves. The stress waves within the material reflects by interaction with the substrate. A transient region of high tensile stress is produced by the interaction of these waves. Simulations suggests that maximum hydrostatic tension which cause failure of polyurea layer is observed in thick coating. Also, the dissipated viscous energy and corresponding temperature rise in a polyurea is calculated, and it is concluded that temperature has influence on deformation.
ContributorsPanwar, Ajay (Author) / Oswald, Jay (Thesis advisor) / Dooley, Kevin (Committee member) / Chen, Kangping (Committee member) / Arizona State University (Publisher)
Created2015
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Description
Recent studies of the occurrence of post-flutter limit cycle oscillations (LCO) of the F-16 have provided good support to the long-standing hypothesis that this phenomenon involves a nonlinear structural damping. A potential mechanism for the appearance of nonlinearity in the damping are the nonlinear geometric effects that arise when the

Recent studies of the occurrence of post-flutter limit cycle oscillations (LCO) of the F-16 have provided good support to the long-standing hypothesis that this phenomenon involves a nonlinear structural damping. A potential mechanism for the appearance of nonlinearity in the damping are the nonlinear geometric effects that arise when the deformations become large enough to exceed the linear regime. In this light, the focus of this investigation is first on extending nonlinear reduced order modeling (ROM) methods to include viscoelasticity which is introduced here through a linear Kelvin-Voigt model in the undeformed configuration. Proceeding with a Galerkin approach, the ROM governing equations of motion are obtained and are found to be of a generalized van der Pol-Duffing form with parameters depending on the structure and the chosen basis functions. An identification approach of the nonlinear damping parameters is next proposed which is applicable to structures modeled within commercial finite element software.

The effects of this nonlinear damping mechanism on the post-flutter response is next analyzed on the Goland wing through time-marching of the aeroelastic equations comprising a rational fraction approximation of the linear aerodynamic forces. It is indeed found that the nonlinearity in the damping can stabilize the unstable aerodynamics and lead to finite amplitude limit cycle oscillations even when the stiffness related nonlinear geometric effects are neglected. The incorporation of these latter effects in the model is found to further decrease the amplitude of LCO even though the dominant bending motions do not seem to stiffen as the level of displacements is increased in static analyses.
ContributorsSong, Pengchao (Author) / Mignolet, Marc P (Thesis advisor) / Chattopadhyay, Aditi (Committee member) / Oswald, Jay (Committee member) / Arizona State University (Publisher)
Created2015
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Description
The football helmet is a device used to help mitigate the occurrence of impact-related traumatic (TBI) and minor traumatic brain injuries (mTBI) in the game of American football. The current design methodology of using a hard shell with an energy absorbing liner may be adequate for minimizing TBI, however it

The football helmet is a device used to help mitigate the occurrence of impact-related traumatic (TBI) and minor traumatic brain injuries (mTBI) in the game of American football. The current design methodology of using a hard shell with an energy absorbing liner may be adequate for minimizing TBI, however it has had less effect in minimizing mTBI. The latest research in brain injury mechanisms has established that the current design methodology has produced a helmet to reduce linear acceleration of the head. However, angular accelerations also have an adverse effect on the brain response, and must be investigated as a contributor of brain injury.

To help better understand how the football helmet design features effect the brain response during impact, this research develops a validated football helmet model and couples it with a full LS-DYNA human body model developed by the Global Human Body Modeling Consortium (v4.1.1). The human body model is a conglomeration of several validated models of different sections of the body. Of particular interest for this research is the Wayne State University Head Injury Model for modeling the brain. These human body models were validated using a combination of cadaveric and animal studies. In this study, the football helmet was validated by laboratory testing using drop tests on the crown of the helmet. By coupling the two models into one finite element model, the brain response to impact loads caused by helmet design features can be investigated. In the present research, LS-DYNA is used to study a helmet crown impact with a rigid steel plate so as to obtain the strain-rate, strain, and stress experienced in the corpus callosum, midbrain, and brain stem as these anatomical regions are areas of concern with respect to mTBI.
ContributorsDarling, Timothy (Author) / Rajan, Subramaniam D. (Thesis advisor) / Muthuswamy, Jitendran (Thesis advisor) / Oswald, Jay (Committee member) / Mignolet, Marc (Committee member) / Arizona State University (Publisher)
Created2014
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Description
Monte Carlo simulations are traditionally carried out for the determination of the amplification of forced vibration response of turbomachine/jet engine blades to mistuning. However, this effort can be computationally time consuming even when using the various reduced order modeling techniques. Accordingly, some investigations in the past have focused on obtaining

Monte Carlo simulations are traditionally carried out for the determination of the amplification of forced vibration response of turbomachine/jet engine blades to mistuning. However, this effort can be computationally time consuming even when using the various reduced order modeling techniques. Accordingly, some investigations in the past have focused on obtaining simple approximate estimates for this amplification. In particular, two of these have proposed the use of harmonic patterns of the blade properties around the disk as an approximate alternative to the many random patterns of Monte Carlo analyses. These investigations, while quite encouraging, have relied solely on single degree of freedom per sector models of the rotor.

In this light, the overall focus of the present effort is a revisit of harmonic

mistuning of rotors focusing first the confirmation of the previously obtained findings with a more detailed model of the blisk in both conditions of an isolated blade-dominated resonance and of a veering between blade and disk dominated modes. The latter condition cannot be simulated by a single degree of freedom per sector model. Further, the analysis will consider the distinct cases of mistuning due to variations of material properties (Young's modulus) and geometric properties (geometric mistuning). In the single degree of freedom model, both mistuning types are equivalent but they are not, as demonstrated here, in more realistic models. The difference arises because changes in geometry induce not only changes in natural frequencies of the blades alone but of their modes and the importance of these two sources of variability is discussed with both Monte Carlo simulation and harmonic mistuning results.

The present investigation focuses also on the possible extension of the harmonic mistuning concept and of its quantitative information that can be derived from such analyses. From it, a novel measure of blade-disk coupling is introduced and assessed in comparison with the coupling index introduced in the past. In conclusions, the low cost of harmonic mistuning computations in comparison with full Monte Carlo simulations is

demonstrated to be worthwhile to elucidate the basic behavior of the mistuned rotor in a random setting.
ContributorsSahoo, Saurav (Author) / Mignolet, Marc Paul (Thesis advisor) / Chattopadhyay, Aditi (Committee member) / Oswald, Jay (Committee member) / Arizona State University (Publisher)
Created2014
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Description
In order to achieve higher gas turbine efficiency, the main gas temperature at turbine inlet has been steadily increased from approximately 900°C to about 1500°C over the last few decades. This temperature is higher than the maximum acceptable temperature for turbine internals. The hot main gas may get ingested into

In order to achieve higher gas turbine efficiency, the main gas temperature at turbine inlet has been steadily increased from approximately 900°C to about 1500°C over the last few decades. This temperature is higher than the maximum acceptable temperature for turbine internals. The hot main gas may get ingested into the space between rotor and stator, the rotor-stator disk cavity in a stage because of the pressure differential between main gas annulus and the disk cavity. To reduce this ingestion, the disk cavity is equipped with a rim seal; additionally, secondary (purge) air is supplied to the cavity. Since the purge air is typically bled off the compressor discharge, this reducing the overall gas turbine efficiency, much research has been carried out to estimate the minimum purge flow necessary (cw,min) for complete sealing of disk cavities.

In this work, experiments have been performed in a subscale single-stage axial turbine featuring vanes, blades and an axially-overlapping radial-clearance seal at the disk cavity rim. The turbine stage is also equipped with a labyrinth seal radially inboard. The stage geometry and the experimental conditions were such that the ingestion into the disk cavity was driven by the pressure asymmetry in the main gas annulus. In the experiments, time-averaged static pressure was measured at several locations in the main annulus and in the disk cavity; the pressure differential between a location on the vane platform close to lip (this being the rim seal part on the stator) and a location in the 'seal region' in the cavity is considered to be the driving potential for both ingestion and egress. Time-averaged volumetric concentration of the tracer gas (CO2) in the purge air supplied was measured at multiple radial locations on the stator surface. The pressure and ingestion data were then used to calculate the ingestion and egress discharge coefficients for a range of purge flow rates, employing a simple orifice model of the rim seal. For the experiments performed, the egress discharge coefficient increased and the ingestion discharge coefficient decreased with the purge air flow rate. A method for estimation of cw,min is also proposed.
ContributorsSingh, Prashant (Author) / Roy, Ramendra P (Thesis advisor) / Mignolet, Marc (Thesis advisor) / Lee, Taewoo (Committee member) / Arizona State University (Publisher)
Created2014
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Description
The focus of this investigation is on the formulation and a validation of reduced order models (ROMs) for the prediction of the response of structures with embedded piezoelectric actuators. The ROMs considered here are those constructed in a nonintrusive manner from a commercial finite element software, NASTRAN is adopted here.

The focus of this investigation is on the formulation and a validation of reduced order models (ROMs) for the prediction of the response of structures with embedded piezoelectric actuators. The ROMs considered here are those constructed in a nonintrusive manner from a commercial finite element software, NASTRAN is adopted here. Notwithstanding the popularity of piezoelectric materials in structural dynamics related applications such as structural health monitoring and energy harvesting, not all commercial finite element software allow directly their modeling. In such cases, e.g., with NASTRAN, one can proceed with an analogy and replace the electric actuation in the piezoelectric material by a fictitious thermal effect producing the same strain. This process recasts the determination of a ROM for a structure with embedded piezoelectric actuator into a similar ROM but for a heated structure, the framework of which has recently been developed. Yet, the temperature field resulting from the analogy would be quite different from the one considered in past effort and would excite a broad array of structural modes. Accordingly, as a preamble to considering a beam with a piezoelectric layer, a simpler plate model is considered that is subjected to a uniform temperature but a complex pressure loading that excites the entire set of modes of the plate in the broad frequency band considered. The very good match of the predictions obtained by this ROM in comparison to their full finite element counterparts provides the necessary confidence to next address a beam with embedded piezoelectic actuator. The test model considered for this validation is a built-up nano beam analyzed recently in nonlinear geometric conditions by full finite elements and by a non-intrusive ROM procedure under harmonic variations of the piezoelectic voltage. This structural model and its loading conditions are very different from those considered in past applications of nonintrusive ROMs, thus the excellent results obtained here provide further support of the broad generality of the nonintrusive ROM methodology, including of the appropriateness of the "dual modes" basis functions.
ContributorsVyas, Varun (Author) / Mignolet, Marc (Thesis advisor) / Hollkamp, Joseph (Committee member) / Liu, Yongming (Committee member) / Arizona State University (Publisher)
Created2014