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Description
Shock loading is a complex phenomenon that can lead to failure mechanisms such as strain localization, void nucleation and growth, and eventually spall fracture. The length scale of damage with respect to that of the surrounding microstructure has proven to be a key aspect in determining sites of failure initiation.

Shock loading is a complex phenomenon that can lead to failure mechanisms such as strain localization, void nucleation and growth, and eventually spall fracture. The length scale of damage with respect to that of the surrounding microstructure has proven to be a key aspect in determining sites of failure initiation. Studying incipient stages of spall damage is of paramount importance to accurately determine initiation sites in the material microstructure where damage will nucleate and grow and to formulate continuum models that account for the variability of the damage process due to microstructural heterogeneity, which is the focus of this research. Shock loading experiments were conducted via flyer-plate impact tests for pressures of 2-6 GPa and strain rates of 105/s on copper polycrystals of varying thermomechanical processing conditions. Serial cross sectioning of recovered target disks was performed along with electron microscopy, electron backscattering diffraction (EBSD), focused ion beam (FIB) milling, and 3-D X-ray tomogrpahy (XRT) to gain 2-D and 3-D information on the spall plane and surrounding microstructure. Statistics on grain boundaries (GB) containing damage were obtained from 2-D data and GBs of misorientations 25° and 50° were found to have the highest probability to contain damage in as-received (AR), heat treated (HT), and fully recrystallized (FR) microstructures, while {111} Σ3 GBs were globally strong. The AR microstructure’s probability peak was the most pronounced indicating GB strength is the dominant factor for damage nucleation. 3-D XRT data was used to digitally render the spall planes of the AR, HT, and FR microstructures. From shape fitting the voids to ellipsoids, it was found that the AR microstructure contained greater than 55% intergranular damage, whereas the HT and FR microstructures contained predominantly transgranular and coalesced damage modes, respectively. 3-D reconstructions of large volume damage sites in shocked Cu multicrystals showed preference for damage nucleation at GBs between adjacent grains of a high Taylor factor mismatches as well as an angle between the shock direction and the GB physical normal of ~30°-45°. 3-D FIB sectioning of individual voids led to the discovery of uniform plastic zones ~25-50% the size of the void diameter and plastic deformation directions were characterized via local average misorientation maps. Incipient transgranular voids revealed from the sectioning process were present in grains of high Taylor factors along the shock direction, which is expected as materials with a low Taylor factor along the shock direction are susceptible to growth due their accomodation of plastic deformation. Fabrication of square waves using photolithography and chemical etching was developed to study the nature of plasticity at GBs away from the spall plane. Grains oriented close to <0 1 1> had half the residual amplitudes than grains oriented close to <0 0 1>.
ContributorsBrown, Andrew (Author) / Peralta, Pedro (Committee member) / Mignolet, Marc (Committee member) / Sieradzki, Karl (Committee member) / Solanki, Kiran (Committee member) / Jiang, Hanqing (Committee member) / Arizona State University (Publisher)
Created2015
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Description
The study of response of various materials to intense dynamic loading events,

such as shock loading due to high-velocity impacts, is extremely important in a wide

variety of military and industrial applications. Shock loading triggers extreme states,

leading to high pressures and strain rates, and neglecting strength is a typical

approximation under such conditions.

The study of response of various materials to intense dynamic loading events,

such as shock loading due to high-velocity impacts, is extremely important in a wide

variety of military and industrial applications. Shock loading triggers extreme states,

leading to high pressures and strain rates, and neglecting strength is a typical

approximation under such conditions. However, recent results have shown that strength

effects are larger than expected, so they must be taken into account. Recently,

hydrodynamic instabilities, the most common being the Rayleigh-Taylor (RTI) and

Richtmyer-Meshkov (RMI) instabilities, have been used to infer the dynamic strength of

materials at high pressure conditions. In our experiments and simulations, a novel RMI

approach is used, in which periodic surface perturbations are made on high purity

aluminium target, which was laser ablated to create a rippled shock front. Due to the

slow linear growth rate of RMI, the evolution of the perturbations on the back surface of

the sample as a result of the rippled shock can be measured via Transient Imaging

Displacement Interferometry (TIDI). The velocity history at the free surface was

recorded by spatially resolved laser velocimetry. These measurements were compared

with the results from the simulations, which were implemented using rate independent

and rate dependent material models, to characterize the dynamic strength of the

material. Simulations using the elastic-perfectly plastic model, which is rate

independent, failed to provide a value of dynamic yield strength that would match

experimental measurements of perturbation amplitudes. The Preston-Tonks-Wallace

(PTW) model, which is rate dependent model, worked well for aluminium. This model

was, in turn, used as a reference for calibrating the rate dependent Steinberg-Lund

model and the results from simulations using the calibration models were also compared

to experimental measurements.
ContributorsGopalakrishnan, Ashish (Author) / Peralta, Pedro (Thesis advisor) / Rajagopalan, Jagannathan (Committee member) / Solanki, Kiran (Committee member) / Arizona State University (Publisher)
Created2017